m-Toluidine → HCID 21388137, compound

HRID 1833989Notes

Reaction equation

HRID 1833989 reaction equation
[CH:1]1[CH:6]=[CH:5][C:4]([O:7][CH2:8][CH2:9]O)=[CH:3][CH:2]=1.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH3:18])[CH:13]=1.P([O-])(OC1C=CC=CC=1)OC1C=CC=CC=1>>[O:7]([CH2:8][CH2:9][NH:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH3:18])[CH:13]=1)[C:4]1[CH:5]=[CH:6][CH:1]=[CH:2][CH:3]=1

Participants

4

Reactant 3

HCID 7934m-ToluidineHCID 31236PhenoxyethanolHCID 23418553Diphenoxyphosphanolate

Product 1

HCID 21388137HCID 21388137, compoundYield 85%

Procedure

138 parts of phenylglycol, 214 parts of m-toluidine and 15 parts of diphenyl phosphite are mixed whilst stirring. The reaction is carried out using the method described in Example 9. 193 parts of N-(2-phenoxyethyl)-m-toluidine, corresponding to a yield of 85% of theory, are obtained at a boiling point of 186° - 192° C/5 mm Hg.

Sources & evidence

ORD record
ord-ad2664c89e42402b94944041dbdad8fc
Source dataset
uspto-grants-1978_01
Patent number
US04067903

Reaction notes

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