HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21388206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | HCID 135840411 | HCID 135840411 | — |
| Product | HCID 21388206 | HCID 21388206 | 60.8% |
Reaction Steps
2-((2-Chlorophenyl)azo)imidazole (20.6 grams; 0.1 mole) was refluxed with 50 cc of methyl iodide in 100 milliters of glyme for 2.0 hours to give 22.0 grams (60.8 percent of theoretical) of 2-((2-chlorophenyl)azo)-1,3-dimethylimidazole iodide melting at 212°-215° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067973 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-2a09748a453c47e9b5a969bfc05625da |
| Source note | uspto-grants-1978_01 |