HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 67838413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 3-Phenoxypyridine | HCID 200510 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67838413 | HCID 67838413 | — |
Reaction Steps
A solution of 9 g. of 3-phenoxypyridine in 20 ml. of absolute ethanol is treated with 9 g. of 70% nitric acid with stirring. The resulting mixture is diluted with 200 ml. of ether and the crystaline precipitate of 3-phenoxypyridine nitrate is collected by filtration, washed with ether and dried at reduced pressure; m.p. 103.5°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067983 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-91ebe2a90d1b464ba4e165a7f4c7dd3b |
| Source note | uspto-grants-1978_01 |