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HRID1834025

反应详情

EQUATION

反应方程式

HRID 1834025 的结构方程式

REACTANTS

反应物

2
结构：CSC(=C[N+](=O)[O-])SC
HCID83623

1-Nitro-2,2-bis(methylthio)ethylene

C4H7NO2S2

结构：NCCCCc1ccccn1
HCID13511083

4-(Pyridin-2-yl)butan-1-amine

C9H14N2

PRODUCTS

生成物

1
结构：CSC(=C[N+](=O)[O-])NCCCCc1ccccn1
HCID70619237

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

2-(4-Aminobutyl)pyridine was reacted with 1-nitro-2,2-bis-methylthio-ethylene in pyridine at 60° for 3.5 hours. Concentration of the reaction mixture and crystallisation yielded 1-nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene, m.p. 78°.

WORKUP

后处理

  1. customConcentration of the reaction mixture and crystallisation