HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 1-Nitro-2-methylamino-2-[4-(2-pyridyl)butylamino]ethylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1-Nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene | HCID 70619237 | — |
| Product | 1-Nitro-2-methylamino-2-[4-(2-pyridyl)butylamino]ethylene | HCID 70619517 | — |
Reaction Steps
A mixture of 1-nitro-2-methylthio-2-[4-(2-pyridyl)butylamino]ethylene and 33% ethanolic methylamine were heated on a steam bath for 15 minutes. Concentration, followed by crystallisation from ethyl acetate yielded the title compound m.p. 90°-91°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067984 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-01ffef5971fc4469a3deab4977c114d8 |
| Source note | uspto-grants-1978_01 |