HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 23666521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | Carbamodithioic acid, N-cyano-, potassium salt (1:2) | HCID 83179 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23666521 | HCID 23666521 | — |
Reaction Steps
A mixture of 80 g of dipotassium N-cyano-dithioimidocarbonate, 64.9 g of p-chlorobenzyl chloride, 400 ml of methanol and 400 ml of water was stirred for 5 hours and the solvents were evaporated. The residue was crystallized from ethanol to obtain monopotassium S-p-chlorobenzyl N-cyano-dithioimidocarbonate with a melting point of 250° C (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04069319 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-4230b3bab14443ed971f5ae51823637b |
| Source note | uspto-grants-1978_01 |