Dimethyl phosphorochloridothionate → HCID 20374672, compound
Reaction equation
[P:1](Cl)([O:5][CH3:6])([O:3][CH3:4])=[S:2].[OH:8][C:9]1[N:13]=[C:12]([S:14][CH2:15][C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][CH:17]=2)[S:11][N:10]=1>>[CH3:4][O:3][P:1]([O:8][C:9]1[N:13]=[C:12]([S:14][CH2:15][C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][CH:17]=2)[S:11][N:10]=1)([O:5][CH3:6])=[S:2]Participants
3
Procedure
Using the procedure of Example 4, dimethyl chlorothiophosphate and 3-hydroxy-5-p-chlorobenzylthio-1,2,4-thiadiazole were reacted to form 3-(dimethoxythiophosphoryloxy) -5-p-chlorobenzylthio-1,2,4-thiadiazole with a refractive index of nD20 = 1.5885.
Workup
- customwere reacted
Sources & evidence
- ORD record
- ord-40758a46ae6b413693b63be57ea583f7
- Source dataset
- uspto-grants-1978_01
- Patent number
- US04069319
Reaction notes
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