HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 178485940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 178433288 | HCID 178433288 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178485940 | HCID 178485940 | 58.8% |
Reaction Steps
A mixture of 4-methyl-5-[(2-aminoethyl)thiomethyl]-imidazole (5.1 g.) and methyl isocyanate (2.0 g.) in acetonitrile was heated for 18 hours in a pressure vessel at 100°. After cooling, the solid obtained was collected and recrystallized from isopropyl alcohol-acetonitrile to give N-methyl-N'-[2-((4-methyl-5-imidazolyl)methylthio)ethyl]urea (4.0 g.) m.p. 158°-159°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04069327 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-ddbff6e3f90345ae847afdfcf814a420 |
| Source note | uspto-grants-1978_01 |