HRID1834321

反应详情

EQUATION

反应方程式

HRID 1834321 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 0.451 g of (S)-(+)-N-salicylidene-1-phenylethylamine, 0.182 g of cupric acetate, 0.7 g of copper powder, 15 ml of cyclohexene, 15 ml of acetonitrile, 5 ml of acetic acid and 5 ml of t-butyl peroxybenzoate was stirred at 20° to 25° C for 6.5 hours in a nitrogen atmosphere. After the reaction, the reaction mixture was treated in the same manner as in Example 1 to obtain 1.60 g of 2-cyclohexenyl acetate.

WORKUP

后处理

  1. customAfter the reaction
  2. additionthe reaction mixture was treated in the same manner as in Example 1