HRID1834325

反应详情

EQUATION

反应方程式

HRID 1834325 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

A mixture of 0.3 g of di-L-prolinato Copper (II), 15 ml of cyclohexene, 20 ml of acetic acid and 5 ml of t-butyl peroxybehzoate was heated with stirring at 90° C for 5 hours in a nitogen atmosphere. After cooling, the reaction mixture was treated in the same manner as in Example 1 to obtain 2.50 g of 2-cyclohexenyl acetate.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureAfter cooling
  3. additionthe reaction mixture was treated in the same manner as in Example 1