HRID1834325
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 90 °C
PROCEDURE
实验过程
A mixture of 0.3 g of di-L-prolinato Copper (II), 15 ml of cyclohexene, 20 ml of acetic acid and 5 ml of t-butyl peroxybehzoate was heated with stirring at 90° C for 5 hours in a nitogen atmosphere. After cooling, the reaction mixture was treated in the same manner as in Example 1 to obtain 2.50 g of 2-cyclohexenyl acetate.
WORKUP
后处理
- temperaturewas heated
- temperatureAfter cooling
- additionthe reaction mixture was treated in the same manner as in Example 1