HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxyethyl 4-methylbenzene-1-sulfonate → N-(2-ethoxyethyl)-2,3,6-trimethyl-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxyethyl 4-methylbenzene-1-sulfonate | HCID 4125390 | — |
| Reactant | 2,3,6-Trimethylaniline | HCID 11958947 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(2-ethoxyethyl)-2,3,6-trimethyl-aniline | HCID 20372930 | 68% |
Reaction Steps
According to the method of Example 1a 553 g (2.26 moles) of p-toluenesulfonic-acid-(2-ethoxyethyl)-ester are added to a solution of 607 g (4.5 moles) 2,3,6-trimethylaniline in 1 liter of toluene. 317 g(68% of theoretical amount) of N-(2-ethoxyethyl)-2,3,6-trimethyl-aniline are obtained, b.p. 150°-152° C / 14 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04070179 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-caa390664d4a4a9691be0a7522983a09 |
| Source note | uspto-grants-1978_01 |