Diazomethane → HCID 3864057, compound

HRID 1834349Notes

Reaction equation

HRID 1834349 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]([CH2:13][C:14]([OH:16])=[O:15])[CH3:12])(=[O:10])=[O:9])=[CH:4][CH:3]=1.[N+](=[CH2:19])=[N-]>>[CH3:19][O:15][C:14](=[O:16])[CH2:13][N:11]([S:8]([C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=1)(=[O:9])=[O:10])[CH3:12]

Participants

3

Reactant 2

HCID 9550DiazomethaneHCID 36274459724-83-3

Product 1

HCID 3864057HCID 3864057, compound

Procedure

2 Parts of N-p-chlorobenzenesulfonyl-sarcosine is added to a diazomethane-ethereal solution. After the generation of nitrogen has ceased, the precipitated reaction product is collected by filtration to obtain 1.2 parts of N-p-chlorobenzenesulfonyl-sarcosine methyl ester, m.p. 80°-80.5° C.

Workup

  1. customthe precipitated reaction product
  2. filtrationis collected by filtration

Sources & evidence

ORD record
ord-004037e4ed1d4ca6a2b8db792028cb25
Source dataset
uspto-grants-1978_01
Patent number
US04070176

Reaction notes

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