HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 2,3,4,5-Tetramethylpyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Hydrogen iodide | HCID 24841 | — |
| Reactant | 2,3-Dimethyl-1H-pyrrole | HCID 39538 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Product | 2,3,4,5-Tetramethylpyrrole | HCID 70484 | 51% |
Reaction Steps
As in Example 58, using 2,3-dimethyl-pyrrole (2 g), acetic acid (50 ml), hydriodic acid (50 ml), hypophosphorous acid (5 ml) and paraformaldehyde (1.2 g). Yield 51%, m.p. 105°-107°. Anal. Found: C, 77.81; H, 10.32; N, 11.45.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04070366 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-0f82ebb6f59d4fde8cd668a440f67c1f |
| Source note | uspto-grants-1978_01 |