Propanal → HCID 53988878, compound
Reaction equation
[CH2:1]([C:3]1[NH:4][C:5]([C:9]([O:11][CH2:12][CH3:13])=[O:10])=[C:6]([CH3:8])[CH:7]=1)[CH3:2].[CH:14](=O)[CH2:15][CH3:16]>>[CH2:1]([C:3]1[NH:4][C:5]([C:9]([O:11][CH2:12][CH3:13])=[O:10])=[C:6]([CH3:8])[C:7]=1[CH2:14][CH2:15][CH3:16])[CH3:2]Participants
3
Procedure
The crude product, obtained as in Example 74 but using 2-ethyl-4-methyl-5-carbethoxypyrrole and propionaldehyde, was sublimed (80° C. 1 × 10-4 mm), m.p. 86°-87° C. (50%).
Workup
- custom(80° C. 1 × 10-4 mm), m.p. 86°-87° C. (50%)
Sources & evidence
- ORD record
- ord-fa735b5f7e0644b980ec44e3b8a1f079
- Source dataset
- uspto-grants-1978_01
- Patent number
- US04070366
Reaction notes
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