Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Benzenepropanal | HCID 7707 | 27% |
Reaction Steps
0.1 g Palladium acetate, 10.2 g iodobenzene, 4.4 g allyl alcohol and 6.0 g triethylamine were heated while stirring under nitrogen to 100° C. After one hour the iodobenzene was 97% reacted and there was produced 27% 3-phenylpropanal and 13% hydratropic aldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04070374 |
|---|
| Source dataset | uspto-grants-1978_01 |
|---|
| ORD ID | ord-30a15c62775045e3925b982a20bb6e92 |
|---|
| Source note | uspto-grants-1978_01 |
|---|
