HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 178433679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | CH2N2Pb | HCID 22262466 | — |
| Reactant | 1,3-bis-[N'-(2-(5-methyl-4-imidazolylmethylthio)ethyl)thioureido] propane | HCID 53759271 | — |
| Product | HCID 178433679 | HCID 178433679 | — |
Reaction Steps
Lead cyanamide (3.0 g) was added to 1,3-bis-[N'-(2-(5-methyl-4-imidazolylmethylthio)ethyl)thioureido]propane (2.5 g) in acetonitrile. Dimethylformamide was added and the mixture was stirred and boiled under reflux for 24 hours. The mixture was filtered, concentrated and purified by chromatography to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04070472 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-a76ca143490842fbadb660823f019a93 |
| Source note | uspto-grants-1978_01 |