Diallylamine → HCID 20324729, compound

Participants

Reaction Steps

A solution was formed containing 19.4 g. of diallylamine in 100 ml. of benzene. Then, 1.57 g. of isobutylsulfonyl chloride was added at such a rate that the temperature did not exceed 45° C. The mixture was stirred and refluxed for 10 minutes, cooled, washed with 100 ml. of dilute hydrochloric acid and then with H2O. It was then dried over magnesium sulfate, filtered and evaporated to give 20.1 g. (02% of theory) of the product, a liquid, nD30 = 1.4697.

Provenance & Evidence