HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 10542413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 70615006 | HCID 70615006 | — |
| Reactant | Jones' reagent | HCID 131709961 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 10542413 | HCID 10542413 | — |
Reaction Steps
To a solution of 3β,19-dihydroxy-5α-androstan-17-one in acetone chilled to 10° C. is added exactly two equivalents of Jones reagent. After standing for 15 minutes the upper acetone layer is poured into water with vigorous stirring. The solid which forms is filtered, air dried and crystallized from hexane to yield 5α-androstane-3,17,19-trione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04071625 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-92f227180abf4c3d98ed613295ef8841 |
| Source note | uspto-grants-1978_01 |