m-Formylbenzonitrile → HCID 9905822, compound

HRID 1835165Notes

Reaction equation

HRID 1835165 reaction equation
[CH3:1][N:2]1[C:7](=[O:8])[C:6]2[CH:9]=[CH:10][O:11][C:5]=2[C:4]([CH2:12][CH:13]([CH3:15])[CH3:14])=[N:3]1.[C:16]([C:18]1[CH:19]=[C:20]([CH:23]=[CH:24][CH:25]=1)[CH:21]=[O:22])#[N:17]>>[OH:22][CH:21]([C:10]1[O:11][C:5]2[C:4]([CH2:12][CH:13]([CH3:15])[CH3:14])=[N:3][N:2]([CH3:1])[C:7](=[O:8])[C:6]=2[CH:9]=1)[C:20]1[CH:23]=[CH:24][CH:25]=[C:18]([C:16]#[N:17])[CH:19]=1

Participants

3

Reactant 2

HCID 90670m-FormylbenzonitrileHCID 23503290HCID 23503290, compound

Product 1

HCID 9905822HCID 9905822, compound

Procedure

Prepared from 5-methyl-7-(2-methylpropyl)furo[2,3-d]pyridazin-4(5H)-one (example 35 step d) and 3-cyanobenzaldehyde following the method of Example 35 step e.

Sources & evidence

ORD record
ord-8024131be8d84b04892446e4ce801f27
Source dataset
uspto-grants-2004_08
Patent number
US06770646B2

Reaction notes

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