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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1835500Generated: November 1, 2026

Dimethylformamide → 2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthalene

https://huagongshe.com/reaction/1835500

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamideHCID 6228—
Reactant2-NaphthalenethiolHCID 7058—
Reactant3,4,5-TrichloronitrobenzeneHCID 88365—
SolventDimethyl SulfoxideHCID 679—
Product2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthaleneHCID 22148877—

Reaction Steps

2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthalene was synthesized (100%) from 3,4,5-trichloronitrobenzene (Acros) and napthalene-2-thiol (Avocado) in a similar manner as described in example 1 using DMSO as solvent instead of DMF.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06770648B2
Source datasetuspto-grants-2004_08
ORD IDord-a27cc8d5e0c54d2da84e21d147eefd20
Source noteuspto-grants-2004_08