HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-1-fluoro-4-nitrobenzene → 2-(2-Chloro-4-nitro-phenylsulfanyl)-5-trifluoromethyl-benzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-1-fluoro-4-nitrobenzene | HCID 67688 | — |
| Reactant | 5-(trifluoromethyl)-1,3-benzothiazole-2-thiol | HCID 178419087 | — |
| Product | 2-(2-Chloro-4-nitro-phenylsulfanyl)-5-trifluoromethyl-benzothiazole | HCID 22148837 | — |
Reaction Steps
2-(2-Chloro-4-nitro-phenylsulfanyl)-5-trifluoromethyl-benzothiazole (252) was prepared (92%) from 2-chloro-1-fluoro-4-nitrobenzene, obtained from Aldrich, and 5-trifluoromethyl-benzothiazol-2-thiol (239) in a similar manner as described in example 251.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06770648B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-bc24fc2d2d594593916a33ca33904488 |
| Source note | uspto-grants-2004_08 |