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HRID1835542

反应详情

EQUATION

反应方程式

HRID 1835542 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1cc([N+](=O)[O-])cc(Cl)c1Sc1nc2cc(C(F)(F)F)ccc2s1
HCID22148876

未命名化合物

结构：O.O.[Cl][Sn]([Cl])([Cl])[Cl]
HCID85782573

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)c1cc(N)cc(Cl)c1Sc1nc2cc(C(F)(F)F)ccc2s1
HCID22148845

未命名化合物

收率 112.2%

PROCEDURE

实验过程

The title compound was prepared using the method of example 270, starting with 1-[3-chloro-5-nitro-2-(5-trifluoromethyl-benzothiazol-2-ylsulfanyl)-phenyl]-ethanone (259) (750 mg, 1.67 mmol), tin chloride dihydrate (Aldrich, 1.89 g, 8.37 mmol). Compound 271 (755 mg, 100%) was obtained as a yellowish solid.

WORKUP

后处理

  1. customThe title compound was prepared