HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-(2-Methyl-benzylidene)-piperidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Product | 1-(2-Methyl-benzylidene)-piperidinium chloride | HCID 17912257 | — |
Reaction Steps
The reaction of 8.5 g (0.100 mol) piperidine and 7.0 g (0.050 mol) 2-chlorobenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.1 g (corresponding to 58% of the yield calculated by theory) 1-(2-methyl-benzylidene)-piperidinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774136B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-74bed366d59c42c6bbc2d7a3f39b0ceb |
| Source note | uspto-grants-2004_08 |