HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| Product | 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride | HCID 22174759 | — |
Reaction Steps
The reaction of 7.3 ml (0.084 mol) morpholine and 5.8 g (0.035 mol) 2,3-dimethoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.1 ml (0.035 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.6 g (corresponding to 59% of the yield calculated by theory) 4-(2,3-dimethoxy-benzylidene)-morpholin-4-ium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774136B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-0aa8e499a1b5440c8ba59139bfaa7af2 |
| Source note | uspto-grants-2004_08 |