HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 4-(2-Methoxy-benzylidene)-morpholin-4-ium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Product | 4-(2-Methoxy-benzylidene)-morpholin-4-ium chloride | HCID 15551911 | — |
Reaction Steps
The reaction of 18.8 ml (0.216 mol) morpholine and 12.4 g (0.09 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 5.3 ml (0.110 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.61 g (corresponding to 38% of the yield calculated by theory) 4-(2-methoxy-benzylidene)-morpholin-4-ium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774136B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-9e0cc563515f4dac90e531e583274370 |
| Source note | uspto-grants-2004_08 |