HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 2-Methoxy-benzylidene-dimethyl-ammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Product | 2-Methoxy-benzylidene-dimethyl-ammonium chloride | HCID 21985303 | — |
Reaction Steps
The reaction of 17.0 ml (0.135 mol) dimethylamine solution and 6.8 ml (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 3.0 ml (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 4.8 g (corresponding to 48% of the yield calculated by theory) (2-methoxy-benzylidene)-dimethyl-ammonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774136B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-222cdeeb719b41fd9a0d50aaba343653 |
| Source note | uspto-grants-2004_08 |