Butanal → HCID 9816600, compound

HRID 1835849Notes

Reaction equation

HRID 1835849 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][C:3]2([C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[NH:8][C:7]2=[O:15])[CH2:2]1.[CH:16](=O)[CH2:17][CH2:18][CH3:19]>>[CH2:16]([N:1]1[CH2:6][CH2:5][CH2:4][C:3]2([C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[NH:8][C:7]2=[O:15])[CH2:2]1)[CH2:17][CH2:18][CH3:19]

Participants

3

Reactant 2

HCID 261ButanalHCID 9859066HCID 9859066, compound

Product 1

HCID 9816600HCID 9816600, compound

Procedure

The compound was prepared according to PROCEDURE 1, Method A by reaction with spiro[indoline-3,3′-piperidin]-2-one and butyraldehyde (10 equiv.). 13C NMR (CDCl3): δ 14.1, 20.6, 21.7, 29.1, 32.0, 49.0, 53.8, 58.5, 58.9, 109.9, 121.9, 126.4, 127.6, 134.9, 140.2, 182.4; MS (TSP): m/z (rel. int.) 260/259 (M+, 25/100).

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-6e5d3e9a4d83481781e6b1a50d810814
Source dataset
uspto-grants-2004_08
Patent number
US06774132B1

Reaction notes

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