Potassium Iodide → HCID 131724519, compound

Participants

Reaction Steps

The compound was prepared according to PROCEDURE 1, Method B by reaction with spiro[indoline-3,3′-piperidin]-2-one and 2-chloroethyl methylether (1.2 equivalents) and potassium iodide (catalytic amount). EtOAc was used for extraction. Yield: 74% 13C NMR (CDCl3): δ 21.8, 31.8, 48.8, 54.2, 58.0, 58.8, 59.2, 70.8, 109.8, 122.0, 126.4, 127.6, 134.8, 140.2, 182.0. The HCl salt was prepared. MS (TSP): m/z (rel. int.) 262/261 (M+, 16/100).

Provenance & Evidence