HCID 13927424, compound → HCID 22179004, compound

HRID 1835968Notes

Reaction equation

HRID 1835968 reaction equation
[CH2:1]([C:3]([OH:10])([CH2:8][CH3:9])[CH2:4][CH2:5][CH2:6][OH:7])[CH3:2].[CH:11]12[CH2:17][CH:14]([CH:15]=[CH:16]1)[CH2:13][CH:12]2[CH2:18][CH2:19][C:20](OC)=[O:21]>>[CH:11]12[CH2:17][CH:14]([CH:15]=[CH:16]1)[CH2:13][CH:12]2[CH2:18][CH2:19][C:20]([O:7][CH2:6][CH2:5][CH2:4][C:3]([CH2:8][CH3:9])([OH:10])[CH2:1][CH3:2])=[O:21]

Participants

3

Reactant 2

HCID 13927424HCID 13927424, compoundHCID 22179015HCID 22179015, compound

Product 1

HCID 22179004HCID 22179004, compoundYield 91%

Procedure

By following the procedure of Synthesis Example 2 except that 4-ethyl-1,4-hexanediol was used instead of 4-methyl-1,4-pentanediol and methyl 3-(5-norbornen-2-yl)propionate used instead of methyl 5-norbornene-2-carboxylate, there was obtained 4-ethyl-4-hydroxyhexyl 3-(5-norbornen-2-yl)propionate. Yield 91%.

Sources & evidence

ORD record
ord-6e840e80633c4ca687d6bd8410efa421
Source dataset
uspto-grants-2004_08
Patent number
US06774258B2

Reaction notes

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