HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citronellal → Cyclohexanol, 5-methyl-2-(1-methylethenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citronellal | HCID 7794 | — |
| Reactant | (-)-Isopulegol | HCID 170833 | — |
| Product | Cyclohexanol, 5-methyl-2-(1-methylethenyl)- | HCID 24585 | 95.1% |
Reaction Steps
In Example 15, isopulegol was synthesized in the same manner as in Example 1, except for replacing d-citronellal with 5.00 g of dl-citronellal. As a result, dl-isopulegol was obtained in a yield of 95.1%, and the ratio of dl-isopulegol to other isomers was 99.4/0.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774269B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-5e4fcff0a5d64276b691bfcc184f4e6c |
| Source note | uspto-grants-2004_08 |