Water → HCID 22608792, compound

HRID 1836069Notes

Reaction equation

HRID 1836069 reaction equation
[I-].[CH:2]1([N+:12]2([CH3:17])[CH2:16][CH2:15][CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[OH2:18]>>[OH-:18].[CH:2]1([N+:12]2([CH3:17])[CH2:16][CH2:15][CH2:14][CH2:13]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 962WaterHCID 22608791HCID 22608791, compound

Product 1

HCID 22608792HCID 22608792, compound

Procedure

N-cyclodecyl-N-methyl-pyrrolidinium iodide (45 gm; 0.128 mol) was dissolved in 150 ml water in a 500 ml plastic bottle. To the solution, 160 gm of Ion-Exchange Resin-OH (BIO RAD® AH1-X8) was added and the mixture was stirred at room temperature overnight. The mixture was filtered and the solids were rinsed with an additional 85 ml of water. The reaction afforded 0.12 mole of the SDA (N-cyclodecyl-N-methyl-pyrrolidinium hydroxide) as indicated by titration analysis with 0.1N HCl.

Workup

  1. filtrationThe mixture was filtered
  2. washthe solids were rinsed with an additional 85 ml of water

Sources & evidence

ORD record
ord-21fa95ba030646a3a679a1c313be6d96
Source dataset
uspto-grants-2004_08
Patent number
US06776973B2

Reaction notes

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