N-Methylhomoveratrylamine → HCID 135493132, compound

Participants

Reaction Steps

89.8 mg (0.46 mmol) of N-methylhomoveratrylamine are added to a solution of 65 mg (0.153 mmol) of the sulfonyl chloride from example IX in 5 ml of dichloromethane. The mixture is stirred overnight at room temperature before the crude product, after concentrating the mixture, is purified by means of preparative TLC chromatography using dichloromethane/methanol 95:5. The oily residue is crystallized with ether.

Provenance & Evidence