HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzoyl Chloride → 4-[3-(4-Methylbenzamidyl)benzoyl]-1-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzoyl Chloride | HCID 13405 | — |
| Reactant | 4-[3-Aminobenzoyl]-1-methylpiperidine | HCID 10130651 | — |
| Product | 4-[3-(4-Methylbenzamidyl)benzoyl]-1-methylpiperidine | HCID 69355584 | 96.1% |
Reaction Steps
Beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (50 mg, 0.229 mmol) and 4-methylbenzoyl chloride (91 μl, 0.687 mmol), 74.0 mg (96%) of the title compound were recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-b63938f5674140d396f7c6d02279dd4f |
| Source note | uspto-grants-2004_08 |