Benzoyl chloride, 3-nitro- → HCID 69354039, compound

HRID 1836378Notes

Reaction equation

HRID 1836378 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[C:5]([CH:7]1[CH2:12][CH2:11][N:10]([CH3:13])[CH2:9][CH2:8]1)=[O:6].[N+:17]([C:20]1[CH:21]=[C:22]([CH:26]=[CH:27][CH:28]=1)[C:23](Cl)=[O:24])([O-:19])=[O:18]>>[N+:17]([C:20]1[CH:21]=[C:22]([CH:26]=[CH:27][CH:28]=1)[C:23]([NH:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[C:5]([CH:7]1[CH2:8][CH2:9][N:10]([CH3:13])[CH2:11][CH2:12]1)=[O:6])=[O:24])([O-:19])=[O:18]

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 101306514-[3-Aminobenzoyl]-1-methylpiperidine

Product 1

HCID 69354039HCID 69354039, compoundYield 21%

Procedure

Beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (50 mg, 0.229 mmol) and 3-nitrobenzoyl chloride (128 mg, 0.687 mmol), 17.4 mg (21%) of the title compound were recovered.

Sources & evidence

ORD record
ord-f761f3779dd8468eafa77d834348e8de
Source dataset
uspto-grants-2004_08
Patent number
US06777428B1

Reaction notes

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