HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Trifluorobenzoyl chloride → 4-[3-(3,4,5-Trifluorobenzamidyl)benzoyl]-1-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Trifluorobenzoyl chloride | HCID 2777023 | — |
| Reactant | 4-[3-Aminobenzoyl]-1-methylpiperidine | HCID 10130651 | — |
| Product | 4-[3-(3,4,5-Trifluorobenzamidyl)benzoyl]-1-methylpiperidine | HCID 23518816 | 99% |
Reaction Steps
Following the example above and beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (25 mg, 0.115 mmol) and 3,4,5-trifluorobenzoyl chloride (30 μL, 0.229 mmol), 42.5 mg (99%) of the title compound were recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-43f3879cfabd408989adf9b201bbebc7 |
| Source note | uspto-grants-2004_08 |