Phenacyl bromide → HCID 22220752, compound

Participants

Reaction Steps

1-(2-Thiazolyl)ethyl acetate (0.8 g, 4.67 mmole) and 2-bromo-1-phenyl-1-ethanone (0.93 g, 4.67 mmole) were combined and stirred at room temp. for 5 days. The viscous mixture was dissolved in acetonitrile (5 mL), diluted with ether (3 mL), and stored overnight at 4 C. The resulting crystals (1.5 g) were recrystallized from acetonitrile/ether to afford 0.97 g of the title compound, mp 155-156 C.

Provenance & Evidence