HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzeneacetic acid, alpha-methyl-, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Phenylpropionic acid | HCID 10296 | — |
| Product | Benzeneacetic acid, alpha-methyl-, ethyl ester | HCID 99643 | — |
Reaction Steps
Dissolve 2-phenylpropionic acid (30 g) in 2B ethanol (100 mL and add anhydrous HCl (10 g). Allow to sit for 48-72 hours, evaporate the solvent in vacuo and purify by distillation to give ethyl 2-phenylpropionate (31 g); bp 100C at 6 mmm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777555B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-cb63f6e801b344d8a00d6b7e20841105 |
| Source note | uspto-grants-2004_08 |