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2-(Bromomethyl)tetrahydro-2H-pyran → 7-Nitro-2-(tetrahydropyran-2-yl)methyl-2h-phthalazin-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Bromomethyl)tetrahydro-2H-pyran | HCID 141917 | — |
| 反応物 | 7-Nitrophthalazin-1(2h)-one | HCID 277729 | — |
| 生成物 | 7-Nitro-2-(tetrahydropyran-2-yl)methyl-2h-phthalazin-1-one | HCID 22180604 | — |
反応手順
Step (b) of Example 125 was repeated, except that the compound prepared in step (b) of Example 137 and tetrahydro-2H-pyran-2-methyl bromide were used as the starting compounds. Thus, 7-nitro-2-(tetrahydropyran-2-yl)methyl-2H-phthalazin-1-one was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06777414B1 |
| 出典データセット | uspto-grants-2004_08 |
| ORD ID | ord-b83091a9fb414ce099dd3e8fe3b6daa6 |
| 出典メモ | uspto-grants-2004_08 |