HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[9-(2,2,2-Trifluoroethylcarbamoyl)-9H-fluoren-9-yl]propyl bromide → ethyl 2-methyly-3-[4-[3-[9-(2,2,2-trifluoroethylcarbamoyl)-9H-fluoren-9-yl]propyl]piperazin-1-yl]-benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[9-(2,2,2-Trifluoroethylcarbamoyl)-9H-fluoren-9-yl]propyl bromide | HCID 10597759 | — |
| Reactant | Ethyl 2-methyl-3-piperazin-1-ylbenzoate | HCID 22180591 | — |
| Product | ethyl 2-methyly-3-[4-[3-[9-(2,2,2-trifluoroethylcarbamoyl)-9H-fluoren-9-yl]propyl]piperazin-1-yl]-benzoate | HCID 86594989 | — |
Reaction Steps
The procedure of step (b) of Example 1 was repeated, except that the compound prepared in step (a) of Example 53 and the compound prepared in step (a) of Example 93 were used as the starting compound. Thus, ethyl 2-methyly-3-[4-[3-[9-(2,2,2-trifluoroethylcarbamoyl)-9H-fluoren-9-yl]propyl]piperazin-1-yl]benzoate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777414B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-d2f8b11cb6254321848b1c5ae0da6690 |
| Source note | uspto-grants-2004_08 |