HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 22390756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22390756 | HCID 22390756 | — |
Reaction Steps
0.163 mol of diethanolamine dissolved in 160 ml of dichloromethane is added, at 10° C., to a solution of 0.168 mol of phenyl isocyanate. After reacting for 1 hour at 10° C. and then for 12 hours at ambient temperature, the reaction mixture is concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06780868B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-caca3859e0c74e6a9e75d961063fc6d5 |
| Source note | uspto-grants-2004_08 |