참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | Zinc | HCID 23994 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Boric acid (HBO2), zinc salt (2:1) | HCID 167155 | — |
반응 단계
An aqueous solution was prepared by dissolving 72.5 g of boric acid (B2O3 content of 56.3%) in 1000 ml of pure water. To the aqueous solution were added 96.0 g of a zinc flower (ZnO content of 99.4%) and 217.5 g of boric acid (B2O3 content of 56.3%), and were stirred and mixed together such that the molar ratio of B2O3/ZnO was 2.0. Next, the solution was stirred and reacted at 60° C. for 90 minutes. The solution was further stirred and reacted at 90° C. for 4 hours. The obtained product was filtered, washed with water and was, then, dried at 105° C. to obtain a zinc borate (sample A-1). Table 3 shows the chemical composition and properties of the thus obtained zinc borate (sample A-1), FIG. 1 shows an X-ray diffraction image thereof, and FIGS. 2 and 3 show electron microphotographs thereof.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06780913B2 |
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| 출처 데이터셋 | uspto-grants-2004_08 |
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| ORD ID | ord-9cf251390bd240e6a5afe5d0fd723c18 |
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| 출처 메모 | uspto-grants-2004_08 |
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