HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 21960155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-(2-Bromoethoxy)Benzaldehyde | HCID 262706 | — |
| Reactant | HCID 135744174 | HCID 135744174 | — |
| Product | HCID 21960155 | HCID 21960155 | 28% |
Reaction Steps
The title compound (1.42 g, 28%) was prepared from 2,5-diethyl-4-methyl-1,6-dihydro-6-pyrimidone (2.70 g, 16.26 mmol) and 4-[2-bromoethoxy]benzaldehyde (4.09 g, 17.86 mmol) in the presence of 95% NaH (508 mg, 20 mmol) as base by a similar procedure to that described in preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06780992B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-677f138a94fb4f21a4cbe934f32d20d7 |
| Source note | uspto-grants-2004_08 |