Hydrochloric Acid → HCID 22677939, compound

Participants

Reaction Steps

To a stirred solution of 1-Boc-4-[(pyrid-4-ylamino)methyl]piperidine (1.0 g, 3.43 mmol) in methanol (100 mL) was added HCl (1 M in ether, 34 mL), and the mixture stirred overnight. The solvent was removed in vacuo, and the resudue taken up in water and freeze dried to give the product as a yellow solid (800 mg, 88%).

Provenance & Evidence