HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178526618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69583690 | HCID 69583690 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178526618 | HCID 178526618 | — |
Reaction Steps
A mixture of 11 g of the product obtained in Step 3, 6 ml of concentrated hydrochloric acid and 150 ml of methanol is heated at reflux for 2 hours. The solvent is concentrated and the residue is taken up in an isopropanol/diethyl ether mixture. The expected product is obtained by filtering off the precipitate that has formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06784183B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-0af9401dae884228ac9b80e269f20f5d |
| Source note | uspto-grants-2004_08 |