HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1837516Generated: October 26, 2026
3-(3-Nitro-phenyl)-acrylonitrile → HCID 22186098, compound
https://huagongshe.com/reaction/1837516
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-(3-Nitro-phenyl)-acrylonitrile | HCID 55669 | — |
| Catalyst | Chlorotris(triphenylphosphine)rhodium(I) | HCID 84599 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22186098 | HCID 22186098 | — |
Reaction Steps
There are introduced into a cylinder 3 g of the product obtained in Step 1, 1.59 g of tris(triphenylphosphine)rhodium(I) chloride and 90 ml of benzene. The whole is heated for 5 hours at 40° C. under a hydrogen pressure of 5 bar. The solvent is evaporated off and the residue is purified by chromatography on silica gel using dichloromethane as eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06784183B2 |
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| Source dataset | uspto-grants-2004_08 |
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| ORD ID | ord-85e8aacf647b40d99e6441bc79a44ef9 |
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| Source note | uspto-grants-2004_08 |
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