HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 12040975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | HCID 15198452 | HCID 15198452 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12040975 | HCID 12040975 | — |
Reaction Steps
[R-(R*,S*)]-β-(Benzoylamino)-α-hydroxybenzenepropanoic acid, ethyl ester (1.16 mmol) is suspended in benzene (10 ml), and triethoxymethane (3.44 mmol) and PPTS (72 mg) are added. Heating to reflux provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06784304B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-7abdcc34df63413a9b7d6a21a5664f26 |
| Source note | uspto-grants-2004_08 |