HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18752451, compound → HCID 16072570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18752451 | HCID 18752451 | — |
| Reactant | HCID 69879159 | HCID 69879159 | — |
| Product | HCID 16072570 | HCID 16072570 | 67.6% |
Reaction Steps
The reaction was carried out in the same manner as in Step 3 of Example 1 using the compound obtained in Step 2 of Example 1 (94 mg) and 3-acetoxy-4-fluoro-2-methylbenzoic acid (45 mg). The resulting crude product was purified by recryatallization from a mixture of EtOAc and n-hexane to obtain the target compound (84 mg, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673772B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-df77c76dae084aec94b13712c6d6ee36 |
| Source note | uspto-grants-2004_01 |