HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2-Methoxy-6-methyl-4-pyridinecarboxylic acid sodium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 2-methoxy-6-methylisonicotinate | HCID 45076200 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Methoxy-6-methyl-4-pyridinecarboxylic acid sodium salt | HCID 69107931 | — |
Reaction Steps
A 6.1 ml portion of 1 N aqueous sodium hydroxide was added to 10 ml of THF containing 1.20 g of 2-methoxy-6-methyl-4-pyridinecarboxylic acid ethyl ester and stirred at room temperature for 1 hour and 20 minutes, and then the reaction solvent was evaporated to obtain 2-methoxy-6-methyl-4-pyridinecarboxylic acid sodium salt. Thereafter, the title compound was obtained by the same procedure of Example 18-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673799B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-4396968ef0554a6c93e51ad6b622e0b2 |
| Source note | uspto-grants-2004_01 |