2-Mepp → HCID 10270095, compound

Participants

Reaction Steps

3-(3-Phenyl-4,5-dihydroisoxazol-5-yl)propanal (27.3 mg, 0.124 mmol), 1-(o-tolyl) piperazine (20.0 mg, 0.113 mmol), molecular sieve (5 beads) and NaBH(OAc)3 (72.1 mg, 0.340 mmol) were reacted in 3 mL of methylene chloride for about 12 hr. With the following processes the same as in Example 1, 30.1 mg (73.1%) of the target compound was obtained.

Provenance & Evidence