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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1838337Generated: October 31, 2026

Potassium Hydroxide → HCID 22504368, compound

https://huagongshe.com/reaction/1838337

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium HydroxideHCID 14797—
ReactantHCID 22504381HCID 22504381—
SolventMethanolHCID 887—
ProductHCID 22504368HCID 2250436890.2%

Reaction Conditions

Temperature60 °C

Reaction Steps

To a mixture solution of the compound obtained in Example 11 (2) (421 mg) in methanol (60 ml), a 1N aqueous potassium hydroxide solution (3 ml) was added and the mixture was stirred at 60° C. for 1 hour. The reaction solution was then concentrated under reduced pressure. The residue was washed with water and ether and dried to obtain 252 mg of the desired product as a yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06673797B1
Source datasetuspto-grants-2004_01
ORD IDord-c3ad217c884545d1a93873abf3b0962c
Source noteuspto-grants-2004_01